带有中间储罐的塔用于间歇萃取精馏

CIESC Journal

• SELECTED PAPERS FROM…… • 上一篇下一篇

带有中间储罐的塔用于间歇萃取精馏

崔现宝; 杨志才; 翟亚锐; 潘玉军

Distillation Laboratory of State Key Laboratories of Chemical Engineering, Tianjin
University, Tianjin 300072,China

收稿日期:1900-01-01 修回日期:1900-01-01 出版日期:2002-10-28 发布日期:2002-10-28
通讯作者: 崔现宝

Batch Extractive Distillation in a Column with a Middle Vessel

CUI Xianbao; YANG Zhicai; ZHAI Yarui; PAN Yujun

Distillation Laboratory of State Key Laboratories of Chemical Engineering, Tianjin
University, Tianjin 300072,China

Received:1900-01-01 Revised:1900-01-01 Online:2002-10-28 Published:2002-10-28
Contact: CUI Xianbao

摘要/Abstract

摘要： Batch extractive distillation was studied in a column with a middle vessel. The process was
simulatedby a constant holdup model and solved by two point implicit method. Acetone and
methanol mixture was separatedin such a setup using water as solvent. The simulation agrees
well with experimental results. The experimental andsimulation results show that the
solvent at the bottom and the product at the top of the column can be
withdrawnsimultaneously for a long period of time. It needs more time for the solvent to
reach high purity than that requiredfor the more volatile component to reach high purity,
so that the time to withdraw solvent from the bottom isdelayed.

关键词: extractive distillation;batch extractive distillation;middle vessel;simulation

Abstract: Batch extractive distillation was studied in a column with a middle vessel. The process was
simulatedby a constant holdup model and solved by two point implicit method. Acetone and
methanol mixture was separatedin such a setup using water as solvent. The simulation agrees
well with experimental results. The experimental andsimulation results show that the
solvent at the bottom and the product at the top of the column can be
withdrawnsimultaneously for a long period of time. It needs more time for the solvent to
reach high purity than that requiredfor the more volatile component to reach high purity,
so that the time to withdraw solvent from the bottom isdelayed.

Key words: extractive distillation, batch extractive distillation, middle vessel, simulation

崔现宝, 杨志才, 翟亚锐, 潘玉军. 带有中间储罐的塔用于间歇萃取精馏[J]. CIESC Journal.

CUI Xianbao, YANG Zhicai, ZHAI Yarui, PAN Yujun. Batch Extractive Distillation in a Column with a Middle Vessel[J]. .

参考文献

[1] Lang, P., Yatim, P., Moszkowicz, P., “Batch extractive distillation under constant
reflux ratio”, Computers Chem.Eng., 18, 1057-1069 (1994).
[2] Lang, P., Lelkes, Z., Moszkowicz, P., “Different operational policies for the batch
extractive distillation”, Computers Chem. Eng., 19, S645-S650 (1995).
[3] Lang, P., Modla, G., Benadda, B., Lelkes, Z., “Homoazeotropic distillation of maximum
azotropes in a batch rectifier with continuous entrainer feeding (I) Feasibility studies”,
Computers Chem. Eng., 24, 1665-1671 (2000).
[4] Lang, P., Modla, G., Kotai, B., Lelkes, Z., Moszkowicz, P.,“Homoazeotropic
distillation of maximum azotropes in a batch rectifier with continuous entrainer feeding (
Ⅱ) Rigorous simulation results”, Computers Chem. Eng., 24,1429-1435 (2000).
[5] Lelkes, Z., Lang, P., Moszkowicz, P., “Batch extractive distillation: The process and
the operational policies”, Chem.Eng. Sci., 53, 1331-1348 (1998).
[6] Lelkes, Z., Lang, P., “Feasibility of extractive distillation in a batch rectifier”,
AIChE J., 44, 810-822 (1998).
[7] Safrit, B.T., Westerberg, A.W., Diwekar, U., Wahnschafft,O.M., “Extending continuous
conventional and extractive distillation feasibility insights to batch distillation”,
Ind.Eng. Chem. Res., 34, 3257-3264 (1995).
[8] Safrit, B.T., Westerberg, A.W., “Improved operational policies for batch extractive
distillation”, Ind. Eng. Chem.Res., 34, 436-443 (1997).
[9] Phimister, J.R., Seider, W., “Semicontinuous, middlevessel, extractive distillation”,
Computers Chem. Eng., 24,879-885 (2000).
[10] Robinson, C.S., Gilliland, E.R., Elements of Fractional Distillation, McGraw Hill Book
Co., New York, 387-388(1950).
[11] Borolo, M., Guarise, G.B., Ribon, N., Rienzi, S., Trotta,A., Macchietto, S., “Some
issues in the design and operation of a batch distillation column with a middle
vessel”,Computers Chem. Eng., 20, S37-S42 (1996).
[12] Barolo, M., Guarise, G.B., Rienzi, S.A., “Running batch distillation in a column with
a middle vessel”, Ind. Eng.Chem. Res., 35, 4612-4618 (1996).
[13] Phimister, J.R., Seider, W.D., “Semicontinuous, middlevessel distillation of ternary
mixtures”, AIChE J., 46,1508-1520 (2000).
[14] Davidyan, A.G., Kiva, V.N., Meski, G.A., “Batch distillation in a column with a
middle vessel”, Chem. Eng. Sci.,49, 3033-3051 (1994).
[15] Meski, G.A., Morari, M., “Design and operation of a batch distillation column with a
middle vessel”, Computers Chem.Eng., 19, S597-S562 (1995).
[16] Cui, X.B., Yang, Z.C., Shao, H.Q., Qu, H.M., “Batch distillation in a cold middle
vessel for heat-sensitive compounds”,Ind. Eng. Chem. Res., 40, 879-884 (2001).

带有中间储罐的塔用于间歇萃取精馏

Batch Extractive Distillation in a Column with a Middle Vessel

PDF (PC)

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 0

编辑推荐

Metrics

本文评价