超临界流体萃取筛板塔中二氧化碳/醇/水体系流体力学特性和传质性能的初步研究

CIESC Journal

超临界流体萃取筛板塔中二氧化碳/醇/水体系流体力学特性和传质性能的初步研究

李德昌,张泽廷,朱美文,于恩平

北京化工学院化工系,北京化工学院化工系,北京化工学院化工系,北京化工学院化工系北京100029.广西化工研究所 ,北京100029 ,北京100029 ,北京100029

出版日期:1993-02-25 发布日期:1993-02-25

STUDY ON HYDRODYNAMICS AND MASS TRANSFER CHARACTERISTICS OF CARBON DIOXIDE / ALCOHOL / WATER SYSTEMS IN A SUPERCRITICAL FLUID EXTRACTION SIEVE - TRAY COLUMN

Li Dechang, Zhang Zeting, Zhu Meiwen and Yu Enping (Department of Chemical Engineering, Beijing Institute of Chemical Technology, Beijing 100029)

Online:1993-02-25 Published:1993-02-25

摘要/Abstract

摘要： 在内径25mm的连续逆流超临界流体萃取筛板塔中,对超临界二氧化碳/乙醇/水和二氧化碳/异丙醇/水2种体系的流体力学特性和传质性能进行了实验研究;对实验数据进行了分析处理,得到了描述超临界流体萃取筛板塔流动特性的关联式,应用柱塞流模型对超临界流体萃取筛板塔的传质性能进行了模拟计算.

Abstract: A study on hydrodynamics and mass transfer characteristics was carried out in acontinuous counter-current sieve - tray extraction column of 25mm in diameter operated in the supercritical solvent region. The supercritical systems studied were carbon dioxide / ethanol / water and carbon dioxide / isopropanol /water. Correlation of all experimental data gave the following flow equation for a supercritical fluid extraction sieve - tray column: Where v=221. 32 m/h, n = 0. 54, m=- 0. 18 for carbon dioxide /ethanol /water system, v=195. 82 m/h, n = 0. 54, m= - 0. 03 for carbon dioxide / isopropanol / water system. The experimental data under steady state were used to estimate the parameters of mass transfer , NOLP , HOLP and KOLa, with a plug - flow model.

李德昌,张泽廷,朱美文,于恩平. 超临界流体萃取筛板塔中二氧化碳/醇/水体系流体力学特性和传质性能的初步研究 [J]. CIESC Journal.

Li Dechang, Zhang Zeting, Zhu Meiwen and Yu Enping (Department of Chemical Engineering, Beijing Institute of Chemical Technology, Beijing 100029). STUDY ON HYDRODYNAMICS AND MASS TRANSFER CHARACTERISTICS OF CARBON DIOXIDE / ALCOHOL / WATER SYSTEMS IN A SUPERCRITICAL FLUID EXTRACTION SIEVE - TRAY COLUMN[J]. .