化工学报 ›› 2005, Vol. 56 ›› Issue (1): 126-129.

• 表面与界面工程 • 上一篇    下一篇

石英光纤表面化学镀镍磷合金工艺

李小甫;姜德生;余海湖;余丁山;杨恩宇;李鸿辉   

  1. 武汉理工大学光纤传感技术研究中心,湖北 武汉 430070
  • 出版日期:2005-01-25 发布日期:2005-01-25

Electroless nickel-phosphor plating process on surface of quartz optical fiber

LI Xiaofu;JIANG Desheng;YU Haihu;YU Dingshan;YANG Enyu;LI Honghui   

  • Online:2005-01-25 Published:2005-01-25

关键词: 石英光纤, 化学镀, 附着力

Abstract: Quartz optical fibers are of great significance in many fields. For example,they can be used to fabricate strain sensors and temperature sensors.If the surface of optical fibers is metal-coated by the electroless plating method, the measuring precision and stability of the optical fiber sensors can be improved remarkably, additionally the life-span of sensors can be prolonged.In this work, an electroless nickel-phosphor plating process for optical fibers was presented.The influences of the content of NaH2PO2•H2O, bath pH value and temperature and the plating deposition rate on the quality of the plating coatings were studied with orthogonal testing.The results indicated that the content of NaH2PO2•H2O was the key factor, which influenced the adhesion force of the plating coatings.The nickel-phosphor plating bath presented in this work possessed excellent stability and the plating deposition rate could be accelerated.Using the process described in this work, nickel-phosphor coatings with great brightness and high adhesion force can be prepared successfully.Optimum conditions were: NiSO4 30 g•L-1, NaH2PO2•H2O 20 g•L-1, C3H6O3 4 ml•L-1, Na2CO3 3 g•L-1, NH4Cl 4 g•L-1, saccharin 1 mg•L-1, temperature 84 ℃, pH 4.6.

Key words: 石英光纤, 化学镀, 附着力