CIESC Journal

• 精细化工 • 上一篇    下一篇

气相色谱内标法测定O,O-二甲基硫代磷酰胺含量

朱 伟 军   

  1. 徐州工业职业技术学院,江苏 徐州 221140
  • 出版日期:2011-12-05 发布日期:2012-03-02

Determination of O,O-dimethyl phosphoramidothioate by GC with an internal standard analysis method

ZHU Weijun   

  1. Xuzhou College of Industrial Technology,Xuzhou 221140,Jiangsu,China
  • Online:2011-12-05 Published:2012-03-02

摘要:

建立了以苯甲酸乙酯为内标物,气相色谱内标法定量测定O,O-二甲基硫代磷酰胺含量的新方法。线性回归方程y=0.6837x+0.0186,相关系数r0.9994,加标回收率达到96.28%,相对标准偏差为1.09%。该方法简便、准确、可靠,适用于O,O-二甲基硫代磷酰胺的质量检验。

Abstract:

A new analysis method for determination of O,O-dimethyl phosphoramidothioate by GC with Ethyl benzoate as internal standard was established. The results were obtained as the linear regression equation of y=0.6837x+0.0186with correlation coefficient r=0.9994. Recovery rate reached 96.28%and RSD was about 1.09%. This method was suitable for quality test of O,O-dimethyl phosphoramidothioate with its simplicityaccuracy and reliability.