• 表面与界面工程 • Previous Articles     Next Articles

PVD AND ITS INCORPORATION WITH ELECTROPLATING TO FABRICATE Fe-C ALLOY FILM OF FIBER OPTICAL CORROSION SENSOR

LUO Yanan;QIU Zhigang;SONG Shizhe;DONG Saying;WANG Hongren;YU hui   

  • Online:2004-06-25 Published:2004-06-25

PVD法及与电镀复合制备光纤腐蚀传感器的Fe-C合金敏感膜

雒娅楠;邱志刚;宋诗哲;董飒英;王洪仁;于辉   

  1. 天津大学材料学院,天津 300072;中国洛阳船舶重工七二五研究所青岛分部,山东 青岛 266071

Abstract: In this paper, a Fe-C alloy corrosion sensing film of the Fiber Optical Corrosion Sensor (FOCS)was fabricated by PVD on the fiber core.The thickness of this film is about 1 μm and the optical signal can respond to the film[DK]’s corrosive information.Furthermore, on the basis of the comparability between the planar wave-guide and column wave-guide,a method of PVD and its incorporation with electroplating was used to fabricate the Fe-C alloy film onto quartz in order to increase the film thickness. The surface morphology of electroplating the Fe-C alloy film was investigated by metallographic microscopy. The structure of film was studied by X-ray diffraction and an electrochemical method was used to evaluate the corrosion resistance of the Fe-C alloy film in NaCl (sodium chloride) solution of different concentration. The initial results showed that the structure and corrosion resistance of the Fe-C alloy film were close to that of carbon steel,and the response between the optical signal and corrosion information of film could be detected. These data have formed the basis of a FOCS.

摘要: 用PVD法制备光纤腐蚀传感器(FOCS)的Fe-C合金敏感膜,在光纤纤芯上得到厚度大约1 μm的Fe-C合金膜,而且光信号对敏感膜的腐蚀信息有响应.为了增加敏感膜的厚度,根据平面波导与圆柱波导的相似性,采用PVD与电镀复合的方法在平板石英玻璃上制备Fe-C合金膜,研究该膜层的形貌、结构和在不同NaCl溶液中的耐蚀性.结果表明:复合制备的Fe-C合金膜的结构和耐蚀性与普通碳钢近似,并初步监测了光信号对敏感膜腐蚀信息的响应,为光纤腐蚀传感器奠定了基础.