CIESC Journal ›› 2006, Vol. 57 ›› Issue (6): 1496-1499.

Previous Articles    

Thermal decomposition dynamics of epoxy adhesive in adhesive/graphite joints

WANG Jun;LIU Wenbin;WANG Chao   

  • Online:2006-06-25 Published:2006-06-25

环氧树脂胶黏剂在石墨粘接接头的热分解动力学

王军;刘文彬;王超   

  1. 哈尔滨工程大学化工学院,黑龙江 哈尔滨 150001;黑龙江省石油化学研究院,黑龙江 哈尔滨 150040

Abstract: The energy dispersive X-ray analysis method can measure the elemental compositions and changes of the epoxy adhesive in adhesive/graphite joints.The weight loss of the adhesive in the adhesive/graphite joint can be measured with EDX, so the thermal decomposition dynamics of the epoxy adhesive in the joint can be determined.The values of thermal decomposition energy of the adhesive in the joint and in the air atmosphere were -35.89 kJ•mol-1 and -34.43 kJ•mol-1,respectively.The rate of thermal decomposition of the adhesive in the joint was lower than that of the adhesive in the air,because air was excluded in the joint.It auord with the rule of thermal decomposition of adhesive.This is a new method of measuring some properties of adhesive in the joints.

Key words: 环氧树脂胶黏剂, 粘接接头, 热分解动力学, X射线能谱

关键词: 环氧树脂胶黏剂, 粘接接头, 热分解动力学, X射线能谱