化工学报 ›› 2012, Vol. 63 ›› Issue (8): 2356-2364.DOI: 10.3969/j.issn.0438-1157.2012.08.004

• 流体力学与传递现象 • 上一篇    下一篇

流量变化对液固流化床瞬态流化特性的影响

尤东光1,2,雍玉梅2,杨超2,张伟鹏2,梁杰1   

  1. 1中国矿业大学(北京)化学与环境工程学院,北京 100083;2中国科学院过程工程研究所绿色过程与工程重点实验室,北京 100190
  • 收稿日期:2012-01-18 修回日期:2012-05-08 出版日期:2012-08-05 发布日期:2012-08-05
  • 通讯作者: 雍玉梅,杨超

Effect of fluidizing flux change on liquid-solids fluidization characteristics

YOU Dongguang1,2,YONG Yumei2,YANG Chao2,ZHANG Weipeng2,LIANG Jie1   

  • Received:2012-01-18 Revised:2012-05-08 Online:2012-08-05 Published:2012-08-05

摘要: 流化床开车、停车及反应控制过程中,对流化床的流量进行调节的不当操作可能致使局部热点的出现,使操作状态恶化,故充分认识流化床的非稳态流化特性具有重要意义。选用直径为0.45 mm的玻璃珠,在厚15 mm、宽400 mm、高1200 mm的二维流化床中进行液固流态化实验,研究了流量变化对颗粒浓度的影响。实验发现,当流量下降时,流化床中形成了浓-稀相突跃界面,且界面前方有过渡段存在;而当流量上升时,流化床中形成的是由浓到稀的过渡段,变化过程中其浓度波动要远大于流量下降时,且需要更长的时间来达到稳定。以相同时间完成流量下降时,流量变化量较小,则流化床各段的平均颗粒浓度变化速度较慢,同时不利于浓-稀相界面的形成。流量下降幅度相等、流量变化时间延长,则使流化床中的颗粒浓度变化速度呈现先慢后快的特点,同时流量变化较慢,则浓-稀相突跃界面不易形成。

关键词: 液固流化床, 流量变化, 操作条件, 流化特性, 固体颗粒浓度

Abstract: The local hot region possibly happening in the fluidized bed under unfavorable operations will lead to deterioration of fluidized states during fluidized beds start up and shut down,so it is important to fully understand the non-steady state of fluidized beds.The experimental study on the effect of fluidizing flux change on solids concentration was carried out in a two-dimensional fluidized bed of 15 mm thickness,400 mm width and 1200 mm height.The glass beads of average diameter of 0.45 mm were chosen as solids phase and water as liquid phase. The experimental results showed that there was an abrupt change of dense-dilute concentration interface with a continuous transition zone in the fluidized bed during the bed collapse process due to decreasing fluidization flux,while there was a continuous dense-dilute concentration interface during the bed expansion process with increasing fluidization flux.The concentration change during the expansion process of fluidized bed was larger than that during the bed collapse process of fluidized bed,and the response time of the expansion process was longer than that of the collapse process. A smaller change of fluid flux in the same time period led to a slower change of average concentration in the bed,which was unfavorable to forming the abrupt change of dense-dilute concentration interface during the collapse process of fluidized bed.A longer time period for the same flux change(slower change of fluidizing flux)led to a slower at first and faster afterwards change of average concentration while it is unfavorable to forming the abrupt change of dense-dilute concentration interface during the collapse process of fluidized bed.

Key words: liquid-solids fluidized bed, fluidizing flux change, operation, fluidization characteristics, solids concentration