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Preparation and Characterization of Silicone Rubber Membrane

LIU Xiujun; LIU Jiaqi; HAN Xu; BAI Yuehua   

  1. School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China
  • Received:1900-01-01 Revised:1900-01-01 Online:2002-10-28 Published:2002-10-28
  • Contact: LIU Xiujun

硅橡胶膜的制备与表征

刘秀军; 刘家祺; 韩煦; 白跃华   

  1. School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China
  • 通讯作者: 刘秀军

Abstract: Pervaporation membrane with preferential permeation for organic compounds over water was
preparedand characterized. Selection of membrane material and the effects of
polydimethylsiloxane (PDMS), cross-linker,and catalyst concentrations on performances of
pervaporation membrane at room temperature were discussed. Inaddition, the time of cross-
linking, and the kinds of basic plate in the process of preparation were tested.
Theformulation of pervaporation membrane material was determined. Through the
characterization of membrane byinfrared spectrometry(IR), scanning electron microscopy
(SEM), transmission electron microscopy(TEM) and Xray diffraction(XRD), it is proved that
the structures and characters are suitable for the pervaporation process.Experiments also
demonstrate that the permeate flux and separation factor are suitable for the process.

Key words: pervaporation membrane, preparation condition, polydimethylsiloxane, characterization

摘要: Pervaporation membrane with preferential permeation for organic compounds over water was
preparedand characterized. Selection of membrane material and the effects of
polydimethylsiloxane (PDMS), cross-linker,and catalyst concentrations on performances of
pervaporation membrane at room temperature were discussed. Inaddition, the time of cross-
linking, and the kinds of basic plate in the process of preparation were tested.
Theformulation of pervaporation membrane material was determined. Through the
characterization of membrane byinfrared spectrometry(IR), scanning electron microscopy
(SEM), transmission electron microscopy(TEM) and Xray diffraction(XRD), it is proved that
the structures and characters are suitable for the pervaporation process.Experiments also
demonstrate that the permeate flux and separation factor are suitable for the process.

关键词: pervaporation membrane;preparation condition;polydimethylsiloxane;characterization