CIESC Journal ›› 2012, Vol. 63 ›› Issue (S1): 28-31.DOI: 10.3969/j.issn.0438-1157.2012.z1.006

Previous Articles     Next Articles

Measurement of diffusion coefficient of water vapor in freeze drying of artifacts

ZHANG Shaozhi1,FANG Yuanyuan1,CHEN Guangming1,LU Heng2   

  • Received:2012-03-27 Revised:2012-03-27 Online:2012-05-28 Published:2012-05-28
  • Supported by:

    prior topic project of Zhejiang Province

文物冷冻干燥水蒸气扩散系数的测量

张绍志1,房圆圆1,陈光明1,卢衡2   

  1. 1浙江大学制冷与低温研究所,浙江 杭州 310027;2浙江省博物馆,浙江 杭州 310007
  • 通讯作者: 陈光明
  • 基金资助:

    浙江省优先主题项目

Abstract: Freeze drying is an effective method to protect unearthed water-logged archaeological wooden artifacts after they are impregnated in polyethylene glycol solution.In this paper,the freeze drying experiments of simulated wooden artifact were carried out on a self-made apparatus.The diffusion coefficient of water vapor in the drying part was fitted according to the experimental data.For a slow cooling velocity of 0.4℃·min-1,the diffusion coefficient was 1.13×10-4m2·s-1;for a quick velocity of 2.0℃·min-1,the diffusion coefficient was 5.53×10-5m2·s-1.The result would offer help for the time prediction and control optimization of the freeze drying of archaeological wooden artifacts.

Key words: freeze drying, archaeological wooden artifacts, diffusion coefficient, water vapor

摘要: 采用聚乙二醇(PEG)溶液进行预处理,然后加以冷冻干燥,是保护出土饱水木质文物的有效方法。在自制的冷冻干燥装置上进行了仿木质文物的冻干实验,根据实验数据拟合得到了干燥区的水蒸气扩散系数。该数据将为文物冻干过程的时间预测和控制优化提供帮助。

关键词: 冷冻干燥, 木质文物, 扩散系数, 水蒸气