Operation properties of oriented grid packing extractor

doi:10.11949/j.issn.0438-1157.20141489

CIESC Journal ›› 2015, Vol. 66 ›› Issue (5): 1792-1797.DOI: 10.11949/j.issn.0438-1157.20141489

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Operation properties of oriented grid packing extractor

FAN Zhaoyun^1,2, CAI Weibin², YANG Yunhui³, WANG Yuqi¹, WANG Yujun², ZHU Shenlin²

1 School of Chemical Engineering, Northwest University, Xi'an 710069, Shaanxi, China;
2 State Key Laboratory of Chemical Engineering, Department of Chemical Engineering, Tsinghua University, Beijing 100084, China;
3 Qidong Julong Petroleum Chemical Equipment Co., Ltd., Qidong 226200, Jiangsu, China

Received:2014-10-07 Revised:2015-02-09 Online:2015-05-05 Published:2015-05-05
Supported by:
supported by the Jiangsu Province Sci-Tech Support Plan (BE2014093).

导向格栅规整填料萃取塔的操作性能

范召运^1,2, 蔡卫滨², 杨蕴辉³, 王玉琪¹, 王玉军², 朱慎林²

1 西北大学化工学院, 陕西西安 710069;
2 清华大学化学工程系, 化学工程联合国家重点实验室, 北京 100084;
3 启东巨龙石油化工装备有限公司, 江苏启东 226200

通讯作者: 王玉琪
基金资助:
江苏省科技支撑计划项目(BE2014093)。

Abstract

Abstract: The hydraulic characteristics and mass transfer efficiency of a new kind of oriented grid packing extractor were investigated by experimental study. The throughput of the new extractor increased greatly than the traditional packed extractor. When velocity ratio L_R (dispersed phase:continuous phase) equaled 1:5, flooding throughout reached 150 m³·m^-²·h^-1. The new packed extractor also exhibited good extraction efficiency, and thus could have excellent application prospects in many areas as solvent deasphalting in petroleum refining process, phenol removal from wastewater in coal chemical industry, etc.

Key words: oriented grid, structured packing, extraction, hydraulic characteristics, mass transfer

摘要： 对一种新开发的导向格栅规整填料萃取塔的水力学特性和传质性能进行了系统的实验研究。结果表明,新型导向格栅填料萃取塔的通量比传统萃取塔有了大幅度的提高,当流速比L_R(分散相:连续相)为1:5时,液泛通量达到150 m³·m^-2·h^-1。该填料萃取塔同时具有较好的传质性能,在石油炼制溶剂脱沥青、煤化工废水萃取脱酚等工业过程有良好的应用前景。

关键词: 导向格栅, 规整填料, 萃取, 水力学特性, 传质

CLC Number:

TQ051.8⁺3

FAN Zhaoyun, CAI Weibin, YANG Yunhui, WANG Yuqi, WANG Yujun, ZHU Shenlin. Operation properties of oriented grid packing extractor[J]. CIESC Journal, 2015, 66(5): 1792-1797.

范召运, 蔡卫滨, 杨蕴辉, 王玉琪, 王玉军, 朱慎林. 导向格栅规整填料萃取塔的操作性能[J]. 化工学报, 2015, 66(5): 1792-1797.

References 21

[1]	Fei Weiyang (费维扬). Progress of study and application on extraction columns [J]. CIESC Journal (化工学报), 2013, 64 (1): 44-51
[2]	Fei Weiyang (费维扬), Ren Zhongqi (任钟旗). Study and application on intensification of extraction columns [J]. Chemical Industry and Engineering Progress (化工进展), 2004, 23 (1): 12-16
[3]	Zhang Huijuan (张慧娟), Wang Henan (王鹤男), Zhang Lühong (张吕鸿), Hao Li (郝丽), Jiang Bin (姜斌). Study on intensification of low interfacial tension system in reciprocating plate extraction column [J]. Chemical Industry and Engineering Progress (化工进展), 2014, 33 (11): 2861-2867
[4]	Zhu Xuanwen (朱璇雯), Liu Cheng (刘成), Zhang Minhua (张敏华). Research status and progress for packed extraction column [J]. Chemical Industry and Engineering Progress (化工进展), 2013, 32 (1): 22-26
[5]	Zhu Shenlin (朱慎林). Development of FG type cellular grid packing and application [J]. Petroleum Refinery Engineering (炼油设计), 1994, 24 (3): 36-40
[6]	Li Jinzhu (李金柱). Operation optimization of the extraction tower of MTBE unit [J]. Petroleum Processing and Petrochemicals (石油炼制与化工), 2008, 39 (1): 53-57
[7]	Qiu Junhong (裘俊红), Chen Guobiao (陈国标), Ji Jianbing (计建炳). Liquid distribution in corrugated sheet structured packed column [J]. Journal of Chemical Industry and Engineering (China) (化工学报), 2003, 54 (5): 646-652
[8]	Jaradat M, Attarakih M, Bart H T. Advanced prediction of pulsed (packed and sieve plate) extraction columns performance using population balance modeling [J]. Chemical Engineering Research and Design, 2011, 89: 2752-2760
[9]	Song Ning (宋宁), Gao Fei (高飞), Liu Chunjiang (刘春江), Huang Zheqing (黄哲庆). Development of efficient extraction packing with gas disturbance [J]. Chemical Engineering (China) (化学工程), 2014, 42 (5): 23-26
[10]	Morales C, Elman H, Perez A. Modeling and simulation of a liquid extraction column with structured packing [J]. Computers & Chemical Engineering, 2007, 31 (12): 1694-1701
[11]	Perez A, Elman H, Morales C. Fluid dynamics study of a liquid-liquid extraction process in a column packed with SMVP [J]. Separation Science and Technology, 2005, 40: 1513-1535
[12]	Owens S A, Perkins M R, Eldridge R B, Schulz K W, Ketcham R A. Computational fluid dynamics simulation of structured packing [J]. I & EC, 2013, 52: 2031-2045
[13]	Zhu Shenlin (朱慎林), Chen Dehong (陈德宏), Fei Weiyang (费维扬). Study on the performance of FG type structured packing extractor [J]. Chemical Engineering (China) (化学工程), 1993, 21 (1): 15-21
[14]	Seibelt A F, Fair J R. Hydrodynamics and mass transfer in spray and packed liquid-liquid extraction column [J]. Ind. Eng. Chem. Res., 1988, 27 (3): 470~481
[15]	Yin Guoyu (尹国玉), Zhang Zeting (张泽廷), Dai Youyuan (戴猷元), Fei Weiyang (费维扬). Structured-packed extraction columns (Ⅰ): Two-phase flow characteristics [J]. Journal of Chemical Industry and Engineering (China) (化工学报), 1991, 42 (3): 289-294
[16]	Zhang Zeting (张泽廷), Yin Guoyu (尹国玉), Fei Weiyang (费维扬), Dai Youyuan (戴猷元). Structured-packed extraction columns (Ⅱ): Mass transfer performance [J]. Journal of Chemical Industry and Engineering (China) (化工学报), 1991, 42 (3): 295-301
[17]	Graler R, Robert N W , Pratt H R C. Liquid-liquid extraction (Ⅳ): A further study of hold-up in packed columns [J]. Trans. Inst. Chem. Eng., 1953, 31: 57-68
[18]	Thornton J D. Science and practice of liquid-liquid extraction (Ⅲ): The effect of pulse wave-form and plate geometry on the performance and throughput of a pulsed column [J]. Trans. Inst. Chem. Eng., 1957, 35: 316-330
[19]	Wang Kiating (汪家鼎), Shen Chunyiao (沈忠耀), Wang Chenfuan (汪承藩). A Preliminary study on two-phasse flow characteristics in pulsed sieve plate column for liquid-liquid extraction [J]. Journal of Chemical Industry and Engineering (China) (化工学报), 1965, 16 (4): 215-220
[20]	Li Jian (李健). The research and measurement about performance of novel extraction packing [D]. Tianjin: Tianjin University, 2007
[21]	Li Zhou (李洲), Li Yigui (李以圭), Fei Weiyang (费维杨), Yang Jichu (杨基础). Liquid-liquid Extraction Process and Equipments (液-液萃取过程和设备) [M]. Beijing: Atomic Energy Press, 1993: 273-274

Operation properties of oriented grid packing extractor

导向格栅规整填料萃取塔的操作性能

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