Higee process intensification technology and application for oceaneering

doi:10.11949/0438-1157.20191374

Abstract

Abstract:

Higee (high gravity) technology, which is carried out in rotating packed bed (RPB), is one of the typical chemical process intensification technologies. Due to its small size, high mass transfer and high separation efficiency, it has been successfully applied in the chemical process on offshore platform. The structure and principle of RPB was introduced, and the related works was summarized in terms of fundamental research, mathematic modeling and CFD simulation of RPB, which provides theoretical support for the wide application of Higee technology. Finally, the industrial application of natural gas dehydration, desulfurization and water deoxidation in the oil and gas production of offshore platforms by supergravity technology is introduced.

Key words: Higee, chemical reactor, gas-liquid flow, mass transfer, oceaneering

摘要：

以旋转填料床（rotating packed bed， RPB）为核心装备的超重力技术是典型的化工过程强化技术之一，由于具有体积小、传质及分离效率高的优点，已被成功应用于海洋平台的化工过程中。介绍了超重力技术的核心装备结构及原理，回顾了针对超重力技术的各项基础实验研究、数学模型化和CFD模拟方面的工作，这些工作为超重力技术的工业应用提供了很好的理论支持。最后介绍了近年来超重力技术在海洋平台油气生产中天然气脱水、脱硫及注入水脱氧过程的工业应用。

关键词: 超重力, 化学反应器, 气液两相流, 传质, 海洋工程

CLC Number:

TQ 028.8

Liangliang ZHANG, Jiwen FU, Yong LUO, Baochang SUN, Haikui ZOU, Guangwen CHU, Jianfeng CHEN. Higee process intensification technology and application for oceaneering[J]. CIESC Journal, 2020, 71(1): 1-15.

张亮亮, 付纪文, 罗勇, 孙宝昌, 邹海魁, 初广文, 陈建峰. 面向海洋工程的超重力过程强化技术及应用[J]. 化工学报, 2020, 71(1): 1-15.

Figures/Tables 17

Fig.1 Structure of different types of rotating packed beds

Fig.2 Liquid phase pattern in cavity zone

Fig.3 Typical images of droplet motion in cavity zone

Fig.4 Dynamic processes of shearing and carrying action with liquid jet impacting on different positions

Fig.5 Liquid holdup maps in wire mesh packing with 18.5, 55.8 and 155.6 mPa?s

Fig.6 Liquid holdup maps in nickel foam packing with 18.5, 55.8，155.6 mPa?s

Table 1 Correlations for estimating gas volumetric mass transfer efficient in different type of RPB

关联式	实验体系及设备类型
$k G = 2.0 a t D G R e 0.7 S c 13 a t d p - 2$	NaOH吸收CO₂，填料塔
$k G = 0.06229 R e G 0.8773 W e L 0.1301 G a 0.07015$	共流型CAS-RPB物理吸收NH₃-H₂O
$k G = 0.01043 R e G 1.0738 W e L 0.1192 G a 0.09007$	逆流型CAS-RPB物理吸收NH₃-H₂O
$k G = 0.08576 R e G 0.8028 W e L 0.1263 G a 0.07637$	共流型SP-RPB物理吸收NH₃-H₂O
$k G = 0.01081 R e G 1.0281 W e L 0.090841 G a 0.09081$	逆流型SP-RPB物理吸收NH₃-H₂O
$k G a e d p D G a t = 0.456 R e L 0.59 R e G 0.63 W e L 0.07 F r - 0.06 σ σ c 0.10$	NaOH吸收SO₂，RPB
$k G a e d p D G a t 2 1 - 0.9 V 0 V t = 0.023 R e L 0.14 R e G 1.13 W e L 0.07 G r G 0.31 a t a p' 1.4$	氨气和VOCs的吸收和解吸，RPB
$k G a e d p D G a t = 0.027 R e L 0.245 R e G 0.679 G r G 0.140$	水脱氧，RPB

Table 1 Correlations for estimating gas volumetric mass transfer efficient in different type of RPB

关联式	实验体系及设备类型
$k G = 2.0 a t D G R e 0.7 S c 13 a t d p - 2$	NaOH吸收CO₂，填料塔
$k G = 0.06229 R e G 0.8773 W e L 0.1301 G a 0.07015$	共流型CAS-RPB物理吸收NH₃-H₂O
$k G = 0.01043 R e G 1.0738 W e L 0.1192 G a 0.09007$	逆流型CAS-RPB物理吸收NH₃-H₂O
$k G = 0.08576 R e G 0.8028 W e L 0.1263 G a 0.07637$	共流型SP-RPB物理吸收NH₃-H₂O
$k G = 0.01081 R e G 1.0281 W e L 0.090841 G a 0.09081$	逆流型SP-RPB物理吸收NH₃-H₂O
$k G a e d p D G a t = 0.456 R e L 0.59 R e G 0.63 W e L 0.07 F r - 0.06 σ σ c 0.10$	NaOH吸收SO₂，RPB
$k G a e d p D G a t 2 1 - 0.9 V 0 V t = 0.023 R e L 0.14 R e G 1.13 W e L 0.07 G r G 0.31 a t a p' 1.4$	氨气和VOCs的吸收和解吸，RPB
$k G a e d p D G a t = 0.027 R e L 0.245 R e G 0.679 G r G 0.140$	水脱氧，RPB

Table 2 Correlations for estimating liquid volumetric mass transfer efficient of different systems

关联式	实验体系
$k L d p D L = 0.9119 S c L 12 R e L 13 a t a 13 G r L 16$	水中氧的解吸，RPB
$k L a e = 0.003689 W e L 0.5476 R e G 0.5449 G r 0.3428$	NaOH吸收CO₂，RPB
$k L a d p D L a t = 0.9 S r L 12 R e L 0.24 G r L 0.29 W e L 0.335$	甘油和CMC脱氧，RPB
$k L a d p D L a t = 8.813 S c L 0.5 G r L 0.37 W e L 0.335$	离子液体捕集CO₂，RPB
$k L a d p D L a t = 0.478 R e L 0.906 G r L 0.275$	水脱氧，RPB
$k L a d p D L a t 1 - 0.93 V 0 V t - 1.13 V i V t = 0.65 S c L 0.5 R e L 0.17 G r L 0.3 W e L 0.3$	水中氧的解吸，RPB
$k L a d p D L a t 1 - 0.93 V 0 V t - 1.13 V i V t = 0.35 S c L 0.5 R e L 0.17 G r L 0.3 W e L 0.3 a t a p' - 0.5 σ c σ w 0.14$	水中氧的解吸，RPB

Table 2 Correlations for estimating liquid volumetric mass transfer efficient of different systems

关联式	实验体系
$k L d p D L = 0.9119 S c L 12 R e L 13 a t a 13 G r L 16$	水中氧的解吸，RPB
$k L a e = 0.003689 W e L 0.5476 R e G 0.5449 G r 0.3428$	NaOH吸收CO₂，RPB
$k L a d p D L a t = 0.9 S r L 12 R e L 0.24 G r L 0.29 W e L 0.335$	甘油和CMC脱氧，RPB
$k L a d p D L a t = 8.813 S c L 0.5 G r L 0.37 W e L 0.335$	离子液体捕集CO₂，RPB
$k L a d p D L a t = 0.478 R e L 0.906 G r L 0.275$	水脱氧，RPB
$k L a d p D L a t 1 - 0.93 V 0 V t - 1.13 V i V t = 0.65 S c L 0.5 R e L 0.17 G r L 0.3 W e L 0.3$	水中氧的解吸，RPB
$k L a d p D L a t 1 - 0.93 V 0 V t - 1.13 V i V t = 0.35 S c L 0.5 R e L 0.17 G r L 0.3 W e L 0.3 a t a p' - 0.5 σ c σ w 0.14$	水中氧的解吸，RPB

Table 3 Correlations for estimating effective mass transfer efficient in literature

关联式	实验体系
$a a t = 1 - e x p - 1.45 σ c σ L 0.75 R e L 0.1 F e L - 0.05 W e L 0.2$	CH₃OH和CCl₄吸收CO₂，填料塔
$a a t = 1.5 σ t d h - 0.5 ρ L u L d h μ L - 0.2 ρ L u L 2 d h σ L 0.75 u L 2 ω 2 r d h - 0.45$	水吸收甘油-空气，填料塔
$a a t = 11906 R e L - 1.8070 F r L - 0.0601 W e L 0.9896$	NaOH吸收CO₂，SP-RPB
$a a t = 54999 R e L - 2.2186 F r L - 0.1748 W e L 1.3160$	NaOH吸收CO₂，SP-RPB
$a a t = 66510 R e L - 1.41 F r L - 0.12 W e L 1.21 c 2 c + d 2 - 0.74$	NaOH吸收CO₂，金属丝网填料，RPB

Table 3 Correlations for estimating effective mass transfer efficient in literature

关联式	实验体系
$a a t = 1 - e x p - 1.45 σ c σ L 0.75 R e L 0.1 F e L - 0.05 W e L 0.2$	CH₃OH和CCl₄吸收CO₂，填料塔
$a a t = 1.5 σ t d h - 0.5 ρ L u L d h μ L - 0.2 ρ L u L 2 d h σ L 0.75 u L 2 ω 2 r d h - 0.45$	水吸收甘油-空气，填料塔
$a a t = 11906 R e L - 1.8070 F r L - 0.0601 W e L 0.9896$	NaOH吸收CO₂，SP-RPB
$a a t = 54999 R e L - 2.2186 F r L - 0.1748 W e L 1.3160$	NaOH吸收CO₂，SP-RPB
$a a t = 66510 R e L - 1.41 F r L - 0.12 W e L 1.21 c 2 c + d 2 - 0.74$	NaOH吸收CO₂，金属丝网填料，RPB

Fig.7 Maldistribution of radial velocity contour plots of gas flow

Fig.8 Streamlines of gas in outer edge of packing zone in RPB

Fig.9 Simulation results about typical liquid flow in an RPB

Fig.10 Liquid forms in two viscosities

Fig.11 Higee device for water deoxidation in Chengdao platform of Shengli oilfield, Sinopec

Fig.12 Offshore oil and gas exploitation ship (a) and Higee device for vacuum water deoxidation (b)

Fig.13 Natural gas desulfurization skid in Nanhai oilfield (a) and Higee desulfurization device (b)

Fig.14 Higee triglycol dehydration device in Bohai platform

References 70

1	胡敏 .《中国油气产业发展分析与展望报告蓝皮书(2018—2019)》正式发布[J]. 炼油技术与工程, 2019, 49(5): 41.
	Hu M . “Bluebook of analysis and outlook report on the development of China s oil and gas industry (2018-2019)” was officially released[J]. Refining Technology and Engineering, 2019, 49(5): 41.
2	李志忠, 赵宏伟, 周昶, 等 . 我国海洋油气开发与未来潜力分析[J]. 中国能源, 2015, 4: 41-44.
	Li Z Z , Zhao H W , Zhou C , et al . China offshore oil and gas production and its potential analysis [J]. Energy of China, 2015, 4: 41-44.
3	Jiao W Z , Liu Y Z , Qi G S . Micromixing efficiency of viscous media in novel impinging stream-rotating packed bed reactor[J]. Ind. Eng. Chem. Res., 2012, 51: 7113-7118.
4	Mohr R J . The role of HIGEE technology in gas processing[R]. USA: Gas Processing Association Meeting, 1985.
5	陈建峰 . 超重力技术及应用: 新一代反应与分离技术[M]. 北京: 化学工业出版社, 2003: 2-50.
	Chen J F . High Gravity Technology and Applications: Next Generation Reaction and Separation Technology [M]. Beijing: Chemical Industry Press, 2003: 2-50.
6	Zhao H , Shao L , Chen J F . High-gravity process intensification technology and application[J]. Chem. Eng. J., 2010, 156: 588-593.
7	Ramshaw C , Mallinson R H . Mass transfer process: US05/963886[P]. 1981.
8	Ramshaw C . “HiGee” distillation - an example of process intensification[J]. Chem. Eng. Lon., 1983, 389: 13-14.
9	俸志荣, 焦纬洲, 余丽胜, 等 . 超重力过程工程装置结构研究进展[J].过程工程学报, 2016, 16(3): 533-540.
	Feng Z R , Jiao W Z , Yu L S , et al . Research progress on structure of supergravity process engineering unit[J]. The Chinese Journal of Process Engineering, 2016, 16(3): 533-540.
10	栗继宏 . 逆流式旋转填料床结构优化设计研究[D]. 太原: 中北大学, 2008.
	Li J H . Research on structural optimization design of counter flow rotating packed bed[D]. Taiyuan: North University of China, 2008: 13-24.
11	陈建峰, 高鑫, 初广文, 等 . 一种多级逆流式超重力旋转床装置: 200920247008.2[P].2009-11-06.
	Chen J F , Gao X , Chu G W , et al . Multi-stage countercurrent supergravity rotating bed device: 200920247008.2[P].2009-11-06.
12	刘有智 . 超重力化工过程与技术[M]. 北京: 国防工业出版社, 2009: 1-5.
	Liu Y Z . Supergravity Chemical Process and Technology[M]. Beijing: National Defense Industry Press, 2009: 1-5.
13	计建炳, 王良华, 徐之超, 等 . 折流式超重力场旋转床装置: 01134321.4[P].2001-10-30.
	Ji J B , Wang L H , Xu Z C , et al . Baffle type supergravity rotating bed device: 01134321.4[P].2001-10-30.
14	计建炳, 徐之超, 俞云良, 等 . 多层折流式超重力旋转床装置:200510049145.1[P].2005-02-24.
	Ji J B , Xu Z C , Yu Y L , et al . Multi-layer baffled supergravity rotating bed device: 200510049145.1[P].2005-02-24.
15	Sandilya P , Rao D P , Sharma A . Gas-phase mass transfer in a centrifugal contactor[J]. Ind. Eng. Chem. Res., 2001, 40(1): 384-392.
16	Chandra A , Goswami P S , Rao D P . Characteristics of flow in a rotating packed bed (HIGEE) with split packing[J]. Ind. Eng. Chem. Res., 2005, 44(11): 4051-4060.
17	潘朝群, 邓先和, 张亚君 . 多级雾化超重力旋转床中气液间的传热[J]. 化工学报, 2005, 56(3): 430-434.
	Pan C Q , Deng X H , Zhang Y J . Heat transfer between gas and liquid in multistage-spraying rotating packed bed [J]. Journal of Chemical Industry and Engineering (China), 2005, 56(3): 430-434.
18	陈昭琼, 熊双喜, 伍极光 . 螺旋型旋转吸收器[J]. 化工学报, 1995, 46(3): 388-392.
	Chen Z Q , Xiong S X , Wu J G , et al . Helical rotating absorber [J]. Journal of Chemical Industry and Engineering (China), 1995, 46(3): 388-392.
19	陈昭琼, 童志权 . 螺旋型旋转吸收器(Ⅱ): 烟气脱硫传质系数[J]. 化工学报, 1996, 47(6): 758-762.
	Chen Z Q , Tong Z Q . Helical rotating absorber (Ⅱ): Mass transfer coefficients of flue gas desulphurization [J]. Journal of Chemical Industry and Engineering (China), 1996, 47(6): 758-762.
20	李友凤, 周继承, 谢放华 . 螺旋通道型旋转床制备纳米拟薄水铝石的研究[J]. 硅酸盐通报, 2006, 2: 38-42.
	Li Y F , Zhou J C , Xie F H . Study on preparation of nanometer pseudo-thin bauxite with spiral channel rotating bed[J]. J. Silicate, 2006, 2: 38-42.
21	Jachuck R J , Lee J , Kolokotsa D , et al . Process intensification for energy saving[J]. Appl. Therm. Eng., 1997, 17(8): 861-867.
22	Jachuck R . Process intensification for responsive processing[J]. Trans. IChemE., 2002, 80(2): 233-238.
23	Vicevic M , Novakovic K , Boodhoo K V K , et al . Kinetics of styrene free radical polymerisation in the spinning disc reactor[J]. Chem. Eng. J., 2008, 135(1): 78-82.
24	Boodhoo K V K , Jachuck R J . Process intensification: spinning disk reactor for styrene polymerisation[J]. Appl. Therm. Eng., 2000, 20(12): 1127-1146.
25	袁渭康, 王静康, 费维扬, 等 . 化学工程手册[M]. 北京: 化学工业出版社, 1983: 2-120.
	Yuan W K , Wang J K , Fei W Y , et al . Chemical Engineering Manual[M]. Beijing: Chemical Industry Press, 1983: 2-120.
26	Woezik B A A V , Westerterp K R . Measurement of interfacial areas with the chemical method for a system with alternating dispersed phases[J]. Chemical Engineering & Processing Process Intensification, 2000, 39(4): 299-314.
27	Jiao W Z , Liu Y Z , Qi G S . Gas pressure drop and mass transfer characteristics in cross-flow rotating packed bed with porous plate packing [J]. Ind. Eng. Chem. Res., 2010, 49(8): 3732-3740.
28	Burns J R , Ramshaw C . Process intensification: visual study of liquid maldistribution in rotation packed beds[J]. Chemical Engineering Science, 2015, 138: 244-255.
29	杨旷, 初广文, 邹海魁, 等 . 旋转床内流体微观流动PIV研究[J]. 北京化工大学学报(自然科学版), 2011, 38(2): 7-11.
	Yang K , Chu G W , Zou H K , et al . PIV study on micro flow of fluid in rotating bed[J]. Journal of BUCT, 2011, 38(2): 7-11.
30	孙润林, 向阳, 杨宇成, 等 . 超重力旋转床液体流动的可视化研究[J]. 高校化学工程学报, 2013, 27(3): 411-416.
	Sun R L , Xiang Y , Yang Y C , et al . Visualization of liquid flow in a supergravity rotating bed[J]. Chem. J. Chinese Universities, 2013, 27(3): 411-416.
31	Sang L , Luo Y , Chu G W , et al . Modeling and experimental studies of mass transfer in the cavity zone of a rotating packed bed[J]. Chem. Eng. Sci., 2017, 170: 355-364.
32	Xu Y C , Li Y B , Liu Y Z , et al . Liquid jet impaction on the single-layer stainless steel wire mesh in a rotating packed bed reactor[J]. AIChE Journal, 2019, 65: e16597.
33	Guo K , Guo F , Feng Y , et al . Synchronous visual and RTD study on liquid flow in rotating packed-bed contactor[J]. Chemical Engineering Science, 2000, 55(9): 1699-1706.
34	李振虎, 郭锴, 翁南梅 . 旋转填充床中两种填料压降特性与传质特性的对比[J]. 北京化工大学学报, 2000, 27(3): 5-8, 12.
	Li Z H , Guo K , Weng N M . Comparison of pressure drop characteristics and mass transfer characteristics of two kinds of packing materials in a rotating packed bed[J]. Journal of BUCT, 2000, 27(3): 5-8, 12.
35	杨旷 . 超重力旋转床微观混合与气液传质特性研究[D]. 北京: 北京化工大学, 2010.
	Yang K . Study on micromixing and gas-liquid mass transfer characteristics of supergravity rotating bed[D]. Beijing: Beijing University of Chemical Technology, 2010.
36	Yang Y , Xiang Y , Chu G , et al . A noninvasive X-ray technique for determination of liquid holdup in a rotating packed bed[J]. Chem. Eng. Sci., 2015, 138: 244-255.
37	Liu Y , Gu D , Xu C , et al . Mass transfer characteristics in a rotating packed bed with split packing[J]. Chin. J. Chem. Eng., 2015, 23: 868-872.
38	Luo Y , Chu G W , Zou H K , et al . Mass transfer studies in a rotating packed bed with novel rotors: chemisorption of CO₂ [J]. Ind. Eng. Chem. Res., 2012, 51: 9164-9172.
39	Guo F , Zheng C , Guo K , et al . Hydrodynamics and mass transfer in cross-flow rotating packed bed[J]. Chem. Eng. Sci., 1997, 52: 3853-3859.
40	Onda K , Sada E , Takeuchi H . Gas absorption with chemical reaction in packed columns[J]. Journal of Chemical Engineering of Japan, 1968, 1: 62-66.
41	Liu Y , Zhang F , Gu D , et al . Gas-phase mass transfer characteristics in a counter airflow shear rotating packed bed[J]. Can. J. Chem. Eng., 2016, 94: 771-778.
42	Su M J , Luo Y , Chu G W , et al . Gas-side mass transfer in a rotating packed bed with structured nickel foam packing[J]. Ind. Eng. Chem. Res., 2018, 57: 4743-4747.
43	Chen Y S . Correlations of mass transfer coefficients in a rotating packed bed[J]. Ind. Eng. Chem. Res., 2011, 50: 1778-1785.
44	Wang Z H , Yang T , Liu Z X , et al . Mass transfer in a rotating packed bed: a critical review[J]. Chemical Engineering & Processing: Process Intensification, 2019, 139: 78-94.
45	Tsai C Y , Chen Y S . Effective interfacial area and liquid-side mass transfer coefficients in a rotating bed equipped with baffles[J]. Separation and Purification Technology, 2015, 144: 139-145.
46	Kumar M P , Rao D P . Studies on a high-gravity gas-liquid contactor[J]. Ind. Eng. Chem. Res., 1990, 29: 917-920.
47	Zhang L L , Wang J X , Xiang Y , et al . Absorption of carbon dioxide with ionic liquid in a rotating packed bed contactor: mass transfer study[J]. Ind. Eng. Chem. Res., 2011, 50: 6957-6964.
48	Lin C C , Jian G S . Characteristics of a rotating packed bed equipped with blade packing[J]. Sep. Purif. Technol., 2007, 54: 51-60.
49	Tung H H , Mah R S H . Modeling liquid mass transfer in higee separation process[J]. Chem. Eng. Commun., 1985, 39: 147-153.
50	Chen Y S , Lin F Y , Lin C C , et al . Packing characteristics for mass transfer in a rotating packed bed[J]. Ind. Eng. Chem. Res., 2006, 45: 6846-6853.
51	Chen Y S , Lin C C , Liu H S . Mass transfer in a rotating packed bed with various radii of the bed[J]. Ind. Eng. Chem. Res., 2005, 44: 7868-7875.
52	Ai T , Mudassar A M , Cai Z , et al . Liquid dispersion and gas absorption in a multi-stage high-speed disperser[J]. Chem. Eng. J., 2018, 352: 704-715.
53	Luo Y , Chu G W , Zou H K , et al . Gas liquid effective interfacial area in a rotating packed bed[J]. Ind. Eng. Chem. Res., 2012, 51: 16320-16325.
54	Rajan S , Kumar M , Ansari M J , et al . Limiting gas liquid flows and mass transfer in a novel rotating packed bed (HiGee) [J]. Ind. Eng. Chem. Res., 2011, 50: 986-997.
55	邹海魁, 初广文, 赵宏, 等 . 面向环境应用的超重力反应器强化技术: 从理论到工业化[J]. 中国科学: 化学, 2014, 44(9): 1413-1422.
	Zou H K , Chu G W , Zhao H , et al . Enhanced technology of supergravity reactors for environmental applications: from theory to industrialization[J]. Scientia Sinaca Chimica, 2014, 44(9): 1413-1422.
56	方健, 詹丽, 余国贤, 等 . 超重力旋转床中气液传质性能的研究进展[J]. 江汉大学学报(自然科学版), 2015, 43(2): 182-187.
	Fang J , Zhan L , Yu G X , et al . Research progress of gas - liquid mass transfer performance in high gravity rotating bed[J]. Journal of Hanjiang University (Natural Science), 2015, 43(2): 182-187.
57	许明, 张建文, 陈建峰, 等 . 超重力旋转床中水脱氧过程的模型化研究[J]. 高校化学工程学报, 2005, 19(3): 309- 314.
	Xu M , Zhang J W , Chen J F , et al . Modeling of water deoxygenation in a rotating packed bed[J]. Chem. J. Chinese Universities, 2005, 19(3): 309- 314.
58	钱智, 徐联斌 . 旋转填充床中伴有可逆反应的气液传质[J]. 化工学报, 2010, 61(4): 832-837.
	Qian Z , Xu J B . Gas-liquid mass transfer accompanied by reversible reaction in rotating packed bed[J]. CIESC Journal, 2010, 61(4): 832-837.
59	Yi F , Zou H K , Chu G W , et al . Modeling and experimental studies on absorption of CO₂ by Benfield solution in rotating packed bed[J]. Chem. Eng. J., 2009, 145: 377-384.
60	Jassim M S , Rochelle G , Eimer D , et al . Carbon dioxide absorption and desorption in aqueous monoethanolamine solutions in a rotating packed bed[J]. Ind. Eng. Chem. Res., 2015, 46: 2823-2833.
61	Llerena-Chavez H , Larachi F . Analysis of flow in rotating packed beds via CFD simulations dry pressure drop and gas flow maldistribution[J]. Chem. Eng. Sci., 2009, 64: 2113-2126.
62	Chen J F , Shao L , Guo F , et al . Synthesis of nano-fibers of aluminum hydroxide in novel rotating packed bed reactor[J]. Chem. Eng. Sci., 2003, 58: 569-575.
63	王洋 . 超重力机内流体流动特性研究[D]. 北京: 北京化工大学, 2016.
	Wang Y . Study on fluid flow characteristics in a supergravity machine[D]. Beijing: Beijing University of Chemical Technology, 2016.
64	Yang Y , Xiang Y , Li Y , et al . 3D CFD modelling and optimization of single-phase flow in rotating packed beds[J]. Can. J. Chem. Eng., 2015, 93: 1138-1148.
65	Liu Y , Luo Y , Chu G W , et al . 3D numerical simulation of a rotating packed bed with structured stainless steel wire mesh packing[J]. Chem. Eng. Sci., 2017, 170: 365-377.
66	Guo T Y , Cheng K P , Wen L X , et al . 3D simulation on liquid flow in a rotating packed bed reactor[J]. Ind. Eng. Chem. Res., 2017, 56: 8169-8179.
67	Ouyang Y , Zou H K , Gao X Y , et al . Computational fluid dynamics modeling of viscous liquid flow characteristics and end effect in rotating packed bed[J]. Chem. Eng. Process., 2018, 123: 185-194.
68	Xie P , Lu X , Yang X , et al . Characteristics of liquid flow in a rotating packed bed for CO₂ capture: a CFD analysis[J]. Chem. Eng. Sci., 2017, 172: 216-229.
69	Lu X , Xie P , Ingham D B , et al . A porous media model for CFD simulations of gas-liquid two-phase flow in rotating packed beds[J]. Chem. Eng. Sci., 2018, 189: 123-134.
70	Ouyang Y , Xiang Y , Gao X Y , et al . Micromixing efficiency in a rotating packed bed with non-Newtonian fluid[J]. Chem. Eng. J., 2018, 354: 162-171.

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