Producing PMMA fibers by electrospinning and model prediction

doi:10.3969/j.issn.0438-1157.2013.05.050

CIESC Journal ›› 2013, Vol. 64 ›› Issue (5): 1869-1875.DOI: 10.3969/j.issn.0438-1157.2013.05.050

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Producing PMMA fibers by electrospinning and model prediction

LI Lu, LI Ruosong, LIU Lingna, FANG Tao

Department of Chemical Engineering, Xi’an Jiaotong University, Xi’an 710049, Shaanxi, China

Received:2012-07-02 Revised:2013-01-30 Online:2013-05-05 Published:2013-05-05
Supported by:
supported by the Research Fund for the Doctoral Program of Higher Education of China(20110201110032),New Teacher Research Support Plan of Xi’an Jiaotong University(08141002)and the International Cooperation Project(2011jdhz37).

静电纺丝技术制备PMMA纤维的分析与模型预测

李璐, 李若松, 刘玲娜, 方涛

西安交通大学化学工程系, 陕西西安 710049

通讯作者: 方涛
作者简介:李璐(1987-),女,博士研究生。
基金资助:
教育部高等学校博士学科点专项科研基金项目(20110201110032);西安交通大学新教师科研支持计划项目(08141002);国际合作项目(2011jdhz37)。

Abstract

Abstract: PMMA fibers were produced by electrospinning from PMMA(poly-methyl-methacrylate)/ethyl acetate solution.Scanning electron microscope(SEM)was used to observe the fibers morphology. The influence of solution concentration, solution flow rate and operating voltage on fiber average diameter was investigated.The Box-Behnken design was used with three main factors, i.e.PMMA solution concentration, solution flow rate and operating voltage.Average diameter of PMMA nanofiber was set as response value.A binary regression model with a high degree of matching the results of experiment was set up by regression analysis.In addition, the results of response surface analysis agreed with univariate analysis results.

Key words: electrospinning, PMMA, response surface methodology, Box-Behnken design

摘要： 以乙酸乙酯为溶剂,对聚甲基丙烯酸甲酯(PMMA)进行静电纺丝以制得PMMA纤维,利用扫描电镜观测其纤维形貌。考察并分析了溶液浓度、流速、接收距离和实验电压对纤维平均直径的影响。利用响应曲面分析中的Box-Behnken design,选取PMMA溶液浓度、流速和实验电压3个因素,以纤维平均直径作为响应值,建立了二元回归模型,且该模型与实验值高度拟合。此外,响应面分析得出的结果与单因素分析一致。

关键词: 静电纺丝, PMMA, 响应曲面法, Box-Behnken design

CLC Number:

TQ340
O631

LI Lu, LI Ruosong, LIU Lingna, FANG Tao. Producing PMMA fibers by electrospinning and model prediction[J]. CIESC Journal, 2013, 64(5): 1869-1875.

李璐, 李若松, 刘玲娜, 方涛. 静电纺丝技术制备PMMA纤维的分析与模型预测[J]. 化工学报, 2013, 64(5): 1869-1875.

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Producing PMMA fibers by electrospinning and model prediction

静电纺丝技术制备PMMA纤维的分析与模型预测

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