从没食子酸结晶母液中回收没食子酸的萃取工艺

doi:10.3969/j.issn.0438-1157.2013.05.022

化工学报 ›› 2013, Vol. 64 ›› Issue (5): 1660-1664.DOI: 10.3969/j.issn.0438-1157.2013.05.022

从没食子酸结晶母液中回收没食子酸的萃取工艺

喻薇, 周康根, 吴运东, 杜虎

中南大学冶金科学与工程学院, 湖南长沙 410083

收稿日期:2012-09-18 修回日期:2012-10-31 出版日期:2013-05-05 发布日期:2013-05-05
通讯作者: 周康根
作者简介:喻薇(1989-),硕士研究生。

Extraction technology for recovery of gallic acid from gallic acid mother liquor

YU Wei, ZHOU Kanggen, WU Yundong, DU Hu

School of Metallurgical Science and Engineering, Central South University, Changsha 410083, Hunan, China

Received:2012-09-18 Revised:2012-10-31 Online:2013-05-05 Published:2013-05-05

摘要/Abstract

关键词: 甲基异丁基酮(MIBK), 没食子酸, 萃取, 反萃

Abstract: A feasible extraction technology is investigated to recover gallic acid from gallic acid mother liquor.It is confirmed that methyl isobutyl ketone(MIBK)is a proper extractant.The influences of initial pH value, gallic acid concentration and phase ratio on extraction efficiency of MIBK are studied in detail.The results show that the pH value of extraction raffinate should be controlled to be less than 2.5 in the extraction process and at about 8 in the stripping process.The extraction rate is improved by increasing the phase ratio.The gallic acid concentration has no obvious effect on the extraction balance in both extraction and stripping processes.The multistage extraction rate reaches 95% at the phase ratio of 1 and the initial pH value of wastewater lower than 2.5.

Key words: methyl isobutyl ketone, gallic acid, extraction, stripping

中图分类号:

TQ202

喻薇, 周康根, 吴运东, 杜虎. 从没食子酸结晶母液中回收没食子酸的萃取工艺[J]. 化工学报, 2013, 64(5): 1660-1664.

YU Wei, ZHOU Kanggen, WU Yundong, DU Hu. Extraction technology for recovery of gallic acid from gallic acid mother liquor[J]. CIESC Journal, 2013, 64(5): 1660-1664.

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从没食子酸结晶母液中回收没食子酸的萃取工艺

Extraction technology for recovery of gallic acid from gallic acid mother liquor

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