CIESC Journal ›› 2019, Vol. 70 ›› Issue (10): 3764-3775.DOI: 10.11949/0438-1157.20190704
• Reviews and monographs • Previous Articles Next Articles
Wei YUAN(),Lingping ZENG,Jianchuan WANG(),Zidong WEI()
Received:
2019-06-21
Revised:
2019-08-13
Online:
2019-10-05
Published:
2019-10-05
Contact:
Jianchuan WANG,Zidong WEI
通讯作者:
王建川,魏子栋
作者简介:
袁伟(1995—),男,硕士研究生,基金资助:
CLC Number:
Wei YUAN, Lingping ZENG, Jianchuan WANG, Zidong WEI. Progress in construction of high efficient ion transport channels for anion exchange membranes fuel cell[J]. CIESC Journal, 2019, 70(10): 3764-3775.
袁伟, 曾玲平, 王建川, 魏子栋. 燃料电池阴离子交换膜高效离子传输通道构建进展[J]. 化工学报, 2019, 70(10): 3764-3775.
Fig.2 TEM pictures of morphology of QCNC in QPPO matrix (a); schematic diagram of ion channels and observed ion channel with TEM, black region representative ion exchange groups (b)[43]
样品 | 填料 | 基膜 | IEC/ (mmol·g-1) | 电导率/ (mS·cm-1) | 吸水率/ % | 应力/ MPa | 文献 |
---|---|---|---|---|---|---|---|
1.0%(mass)QN-PAEK/rGO | rGO | QN-PAEK | 1.57 | 115@90℃ | 75@30℃ | 29.0 | [ |
QPVA/0.1%Fe3O4-GO with magnetic | Fe3O4-GO | QPVA | — | 54.4@60℃ | — | 40.0 | [ |
QTNT/QPSU | QTNT | QPSU | 1.73 | 19.5@RT | 16.2@RT | 40.0 | [ |
QPSF/5% LDH | LDH | QPSF | — | 23.6@RT | 20.5@60℃ | 17.5 | [ |
PVA/DGBE-15/SiO2-3 | DGBE 和 SiO2 | PVA | 1.10 | 4.2@25℃ | 48.3@25℃ | 20.7 | [ |
QPSF/5%MMT-1 | 功能化蒙脱土 | QPSF | 1.21 | 47.3@95℃ | 102@95℃ | 26.7 | [ |
QPPO/6%palygorskite | 坡缕石 | QPPO | 1.07 | 21.5@80℃ | 37.4@20℃ | 28.0 | [ |
10%CQPVA-CL | 壳聚糖 | QPVA | 1.09 | 27@70℃ | — | — | [ |
QPPO/QCNC (2%) | 季铵化纤维素 | QPPO | 1.05 | 28@20℃ | 16.9@20℃ | 30.9 | [ |
Table 1 Comprehensive properties of some nanocomposite membranes
样品 | 填料 | 基膜 | IEC/ (mmol·g-1) | 电导率/ (mS·cm-1) | 吸水率/ % | 应力/ MPa | 文献 |
---|---|---|---|---|---|---|---|
1.0%(mass)QN-PAEK/rGO | rGO | QN-PAEK | 1.57 | 115@90℃ | 75@30℃ | 29.0 | [ |
QPVA/0.1%Fe3O4-GO with magnetic | Fe3O4-GO | QPVA | — | 54.4@60℃ | — | 40.0 | [ |
QTNT/QPSU | QTNT | QPSU | 1.73 | 19.5@RT | 16.2@RT | 40.0 | [ |
QPSF/5% LDH | LDH | QPSF | — | 23.6@RT | 20.5@60℃ | 17.5 | [ |
PVA/DGBE-15/SiO2-3 | DGBE 和 SiO2 | PVA | 1.10 | 4.2@25℃ | 48.3@25℃ | 20.7 | [ |
QPSF/5%MMT-1 | 功能化蒙脱土 | QPSF | 1.21 | 47.3@95℃ | 102@95℃ | 26.7 | [ |
QPPO/6%palygorskite | 坡缕石 | QPPO | 1.07 | 21.5@80℃ | 37.4@20℃ | 28.0 | [ |
10%CQPVA-CL | 壳聚糖 | QPVA | 1.09 | 27@70℃ | — | — | [ |
QPPO/QCNC (2%) | 季铵化纤维素 | QPPO | 1.05 | 28@20℃ | 16.9@20℃ | 30.9 | [ |
样品 | 方法 | IEC/ (mmol·g-1) | 电导率/ (mS·cm-1) | 吸水率/% | 溶胀率/% | 应力/ MPa | 文献 |
---|---|---|---|---|---|---|---|
PSf–PDApip4 | 嵌段共聚 | 2.02 | 102@80℃ | 45.4@80℃ | — | 21.0 | [ |
NCBP-Im | 嵌段共聚 | 1.25 | 35.0@RT | 13.3@RT | 4.5@RT | 28.5 | [ |
PPO51-Im0.78F0.3 | 侧链接枝 | 1.16 | 15.9@30℃ | 12.5@30℃ | 3.0@30℃ | 24.1 | [ |
ImPEK-0.4 | 侧链接枝 | 1.68 | 83.6@80℃ | 17.9@80℃ | 7.9@80℃ | 69.6 | [ |
x(QH)3QPPO-40 | 侧链接枝 | 3.59 | 110@80℃ | — | 25@80℃ | 20.0 | [ |
M-OH-1∶1 | 侧链接枝 | 1.88 | 14.9@RT | 6.5@RT | 4.9 | 35.0 | [ |
PAEK-PIL0.8 | 侧链接枝 | 2.05 | 49.4@RT | 15.5@RT | 12.1 | 11.6 | [ |
PK-QD-54 | 侧链接枝 | 2.02 | 36.6@30℃ | 21.6@30℃ | 8.4@30℃ | 30.0 | [ |
Table 2 Comprehensive properties of microphase separation membranes
样品 | 方法 | IEC/ (mmol·g-1) | 电导率/ (mS·cm-1) | 吸水率/% | 溶胀率/% | 应力/ MPa | 文献 |
---|---|---|---|---|---|---|---|
PSf–PDApip4 | 嵌段共聚 | 2.02 | 102@80℃ | 45.4@80℃ | — | 21.0 | [ |
NCBP-Im | 嵌段共聚 | 1.25 | 35.0@RT | 13.3@RT | 4.5@RT | 28.5 | [ |
PPO51-Im0.78F0.3 | 侧链接枝 | 1.16 | 15.9@30℃ | 12.5@30℃ | 3.0@30℃ | 24.1 | [ |
ImPEK-0.4 | 侧链接枝 | 1.68 | 83.6@80℃ | 17.9@80℃ | 7.9@80℃ | 69.6 | [ |
x(QH)3QPPO-40 | 侧链接枝 | 3.59 | 110@80℃ | — | 25@80℃ | 20.0 | [ |
M-OH-1∶1 | 侧链接枝 | 1.88 | 14.9@RT | 6.5@RT | 4.9 | 35.0 | [ |
PAEK-PIL0.8 | 侧链接枝 | 2.05 | 49.4@RT | 15.5@RT | 12.1 | 11.6 | [ |
PK-QD-54 | 侧链接枝 | 2.02 | 36.6@30℃ | 21.6@30℃ | 8.4@30℃ | 30.0 | [ |
样品 | 非离子聚合物网络 | 离子聚合物网络 | IEC/ (mmol·g-1) | 电导率/ (mS·cm-1) | 吸水率/% | 溶胀度/% | 应力/MPa | 文献 |
---|---|---|---|---|---|---|---|---|
PBI/DAIm TIPN-65/0.5 | PBI | P[DAIm] | 0.63 | 96.7@80℃ | 23.0 | 4.4 | 48.2 | [ |
PVA/30%PPO | PVA | QPPO | 1.29 | 151@RT | 67.0 | 26.0 | 41 | [ |
SIPN-60-2 | xPEG-PAGE | QAPPO | 1.43 | 67.7@80℃ | 96.5 | 17.4 | 93.4 | [ |
VPPO/VBC(2.0)-IPN | PPO | PVBC | 1.82 | 69.7@90℃ | 1.2 | ~0 | >35 | [ |
sIPN-62/30 | PPO-N3 | CM-PS | 1.44 | 97.8@80℃ | 68.8 | 12.0 | 11.3 | [ |
pp-50 | PVA-GA | PVBC-c-PVIm | 1.86 | 21.9@30℃ | 39.4 | 28.6 | 36.7 | [ |
IPN64 | PVA-GA | QPSF | 1.13 | 18.2@60℃ | 30 | 12 | 12.7 | [ |
Table 3 Comprehensive properties of interpenetrating polymer network membranes
样品 | 非离子聚合物网络 | 离子聚合物网络 | IEC/ (mmol·g-1) | 电导率/ (mS·cm-1) | 吸水率/% | 溶胀度/% | 应力/MPa | 文献 |
---|---|---|---|---|---|---|---|---|
PBI/DAIm TIPN-65/0.5 | PBI | P[DAIm] | 0.63 | 96.7@80℃ | 23.0 | 4.4 | 48.2 | [ |
PVA/30%PPO | PVA | QPPO | 1.29 | 151@RT | 67.0 | 26.0 | 41 | [ |
SIPN-60-2 | xPEG-PAGE | QAPPO | 1.43 | 67.7@80℃ | 96.5 | 17.4 | 93.4 | [ |
VPPO/VBC(2.0)-IPN | PPO | PVBC | 1.82 | 69.7@90℃ | 1.2 | ~0 | >35 | [ |
sIPN-62/30 | PPO-N3 | CM-PS | 1.44 | 97.8@80℃ | 68.8 | 12.0 | 11.3 | [ |
pp-50 | PVA-GA | PVBC-c-PVIm | 1.86 | 21.9@30℃ | 39.4 | 28.6 | 36.7 | [ |
IPN64 | PVA-GA | QPSF | 1.13 | 18.2@60℃ | 30 | 12 | 12.7 | [ |
样品 | IEC/ (mmol·g-1) | 离子簇/nm | 电导率/ (mS·cm-1) | 吸水率/ % | 溶胀度/ % | 应力/ MPa | 文献 |
---|---|---|---|---|---|---|---|
Di-DQP-OH | 2.45 | 2.00 | 46.8@30℃ | 49.5 | — | — | [ |
C-HPPES-4/1 | 1.83 | 16.03 | 143.4@80℃ | 31.7 | 11.3 | 39.7 | [ |
PQA-PPAEK | 2.17 | — | 11.1@20℃ | 9.3 | — | 17.9 | [ |
PAES-15-IMPPO | 2.55 | 15.00 | 78.8@80℃ | 119.6 | 28.0 | 36.0 | [ |
QBPES-60 | 1.93 | 8.26 | 40.5@60℃ | 42.6 | 7.8 | 26.4 | [ |
PI-ran-P[VBTMA][Cl] 2.15 | 1.42 | 5.20 | 19.6@60℃ | 67.3 | — | — | [ |
ImPESN-19-22 | 2.07 | 17.95 | 146.7@80℃ | 18.4 | 25.5 | 31.7 | [ |
QPSU-3%QPOSS | 1.65 | 20.00 | 53.6@80℃ | 61.8 | 23.0 | 36.6 | [ |
Table 4 Comprehensive properties of AEMs with ion clusters
样品 | IEC/ (mmol·g-1) | 离子簇/nm | 电导率/ (mS·cm-1) | 吸水率/ % | 溶胀度/ % | 应力/ MPa | 文献 |
---|---|---|---|---|---|---|---|
Di-DQP-OH | 2.45 | 2.00 | 46.8@30℃ | 49.5 | — | — | [ |
C-HPPES-4/1 | 1.83 | 16.03 | 143.4@80℃ | 31.7 | 11.3 | 39.7 | [ |
PQA-PPAEK | 2.17 | — | 11.1@20℃ | 9.3 | — | 17.9 | [ |
PAES-15-IMPPO | 2.55 | 15.00 | 78.8@80℃ | 119.6 | 28.0 | 36.0 | [ |
QBPES-60 | 1.93 | 8.26 | 40.5@60℃ | 42.6 | 7.8 | 26.4 | [ |
PI-ran-P[VBTMA][Cl] 2.15 | 1.42 | 5.20 | 19.6@60℃ | 67.3 | — | — | [ |
ImPESN-19-22 | 2.07 | 17.95 | 146.7@80℃ | 18.4 | 25.5 | 31.7 | [ |
QPSU-3%QPOSS | 1.65 | 20.00 | 53.6@80℃ | 61.8 | 23.0 | 36.6 | [ |
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