聚碳酸酯液液分离器的流体力学模拟和中试试验

doi:10.3969/j.issn.0438-1157.2013.06.029

化工学报 ›› 2013, Vol. 64 ›› Issue (6): 2109-2116.DOI: 10.3969/j.issn.0438-1157.2013.06.029

聚碳酸酯液液分离器的流体力学模拟和中试试验

程华农^1,2, 刘群山¹, 王炳强¹, 郑世清^1,2, 付振波³

1. 青岛科技大学计算机与化工研究所,山东青岛 266042;
2. 兵器集团公司聚氨酯研发中心, 山东青岛 266042;
3. 甘肃银光化学工业集团有限公司,甘肃白银 730900

收稿日期:2012-09-18 修回日期:2013-01-08 出版日期:2013-06-05 发布日期:2013-06-05
通讯作者: 程华农(1974—),男,博士,副研究员。
作者简介:程华农(1974—),男,博士,副研究员。
基金资助:
兵器工业集团科技开发项目(20103702001902,20103702001578,20103702001622)。

Fluid dynamics simulation and pilot test for polycarbonate liquid-liquid separator

CHENG Huanong^1,2, LIU Qunshan¹, WANG Bingqiang¹, ZHENG Shiqing^1,2, FU Zhenbo³

1. Research Center of Computer and Chemical Engineering, Qingdao University of Science and Technology, Qingdao 266042, Shandong, China;
2. Polyurethane Research Center of China North Industries Group Corporation, Qingdao 266042, Shandong, China;
3. Gansu Yinguang Chemical Industry Group Co., Ltd., Baiyin 730900, Gansu, China

Received:2012-09-18 Revised:2013-01-08 Online:2013-06-05 Published:2013-06-05
Supported by:
supported by the Foundation of China North Industries Group Corporation(20103702001902,20103702001578,20103702001622).

摘要/Abstract

摘要： 对聚碳酸酯混合液,通过液液间歇沉降实验得到分散相液滴的Sauter平均粒径为330 μm。采用Mixture多相流模型对聚碳酸酯液液静态分离器进行了模拟和分析。对平行板、波纹板和斜板进行了比较,得出斜板更适合聚碳酸酯液液分离。考察了斜板长、板间距、倾斜角度、入口流量对液液分离效果的影响,得出对于水油相体积比为0.6的物料,最优的聚结板参数为斜板倾角20°、板长0.8 m、板间距40 mm、筒内最大流速5.3×10^-3 m·s^-1。设计了聚碳酸酯液液分离器,进行了中试试验,水油两相出口浓度接近各自的溶解度值,筒内最大流速为3.9×10^-3 m·s^-1,结果表明该分离器起到了很好的液液分离效果,可以取代原有的碟片离心机设备,降低了设备和操作费用。

关键词: 聚碳酸酯, 液液分离器, 斜板, 流体力学

Abstract: The calculated Sauter average drop size of the dispersed phase is 330 μm in the liquid-liquid static settlement experiment for the polycarbonate mixture.The liquid-liquid separation process is simulated and analyzed using mixture multiphase flow model.Different types of coalescence plates are compared, including parallel plates, corrugated plates and inclined plates.The results show that inclined plates are more suitable to the polycarbonate liquid-liquid separation.For the water-oil volume ratio of 0.6, the optimal parameters for the inclined plates are:inclined angle 20°, board length 0.8 m, and plate spacing 40 mm.The maximal flow rate in the separator is 5.3×10^-3 m·s^-1.According to the calculation results, a polycarbonate liquid-liquid separator is designed and applied in the pilot scale test, which presents a good separation effect.The concentration of water/oil phases is close to the solubility.The maximal material flow rate in the actual liquid-liquid separator is 3.9×10^-3 m·s^-1.The common disc centrifuges can be replaced by the designed static separators, reducing the cost of equipment and operation greatly.

Key words: polycarbonate, liquid-liquid separator, inclined plate, fluid dynamics

中图分类号:

TQ028.4

程华农, 刘群山, 王炳强, 郑世清, 付振波. 聚碳酸酯液液分离器的流体力学模拟和中试试验[J]. 化工学报, 2013, 64(6): 2109-2116.

CHENG Huanong, LIU Qunshan, WANG Bingqiang, ZHENG Shiqing, FU Zhenbo. Fluid dynamics simulation and pilot test for polycarbonate liquid-liquid separator[J]. CIESC Journal, 2013, 64(6): 2109-2116.

参考文献 23

[1]	Yang Ruxin(杨茹欣), Niu Chengxiang(牛承详).New progress of PC process and products development[J].Chemical Techno-Economics(化工技术经济), 2005(10):31-33
[2]	Cheng Huanong(程华农), Wang Bingqiang(王炳强), He Yaping(何亚平), Zheng Shiqing(郑世清), Fu Zhenbo(付振波).Experimental study on polycarbonate glue washing process[J].Chemical Engineering(China)(化学工程), 2010,40(1):73-78
[3]	Inada M, Abe H, Taguchi M.Preparation of polycarbonate glue:CN,01434695A.2009-5-20
[4]	Gool van C A M, Oyevaar M H, Warren A, Tinney C, Zhu M.Process for the purification of polycarbonate containing solutions by plate decantation[P]:CN,100358934C. 2008-1-2
[5]	Richard B, Christian K, Lora R, Jurgen H.Purification of solutions containing polycarbonate[P]:US, 6458920B1. 2002-10-1
[6]	Sun Zhiqian(孙治谦),Wang Zhenbo(王振波),Jin Youhai(金有海), Guo Dong(郭栋).Numerical research of oil-water gravity separator[J].Industrial Water Treatment(工业水处理), 2010,30(1):69-72
[7]	Zhou Yong(周永), Wu Yingxiang(吴应湘), Zheng Zhichu(郑之初), Liu Qiusheng(刘秋生),Li Qingping(李清平).Research on oil-water separation technique(Ⅰ):Numerical simulation in both straight and helical pips[J].Journal of Hydrodynamics(水动力学研究与进展), 2004,19(4):540-546
[8]	Tang Hongtao(唐洪涛), Wu Jianhua(吴剑华).Study of theoretical plate length on the inclined plate separator[J].Fluid Machinery(流体机械), 2005,33(10):20-23
[9]	Lü Yuling(吕宇玲), He Limin(何利民), Wang Guodong(王国栋), Ni Lingying(倪玲英).Numerical simulation of flow field inside gravitational separator with different internals[J].China Petroleum Machinery(石油机械), 2008,36(2):12-16
[10]	Cheng Huanong(程华农), Liu Qunshan(刘群山),Wang Bingqiang(王炳强), Zheng Shiqing(郑世清).Fluid dynamics simulation of inlet internals in polycarbonate liquid-liquid separator[J].Computers and Applied Chemistry(计算机与应用化学), 2012,29(2):132-136
[11]	Frankiewicz T, Lee C M.Using computational fluid dynamics(CFD)simulation to model fluid motion in process vessels on fixed and floating platforms[J].Soc.Petroleum Eng.,2002:1-9
[12]	Pourahmadi L A.CFD simulation of multiphase separators.Calgary, Canada:University of Calgary,2010
[13]	Wang Bingqiang(王炳强).Study on PC washing process.Qingdao:Qingdao University of Science and Technology, 2012
[14]	Olila O G, Reddy K R.Phosphorus sorption characteristics of sediments in two eutrophic lakes in Florida[J].Arch Hydrobiol., 1993,129:45-65
[15]	Torrent J, Schwertmann U, Barron V.Fast and slow phosphorus sorption by goethite-rich natural materials[J].Clay and Clay Minerals, 1992,40:14-21
[16]	Martin H, Lars H.Determination of a coalescence parameter from batch-settling experiments[J].Chemical Engineering Journal, 2002(85):369-378
[17]	Wang Xuewen(王学文), Zheng Yuanyang(郑远扬).Study on high effective closed oil-water separator application[J].Industrial Water Treatment(工业水处理), 1995,15(1):29-31
[18]	Cao Jianshu(曹建树), Li Weiqing(李卫清), Zheng Yuanyang(郑远扬).Research and application of new oil-water separator with corrugated plate packing[J].Fluid Machinery(流体机械),2005,33(9):1-3
[19]	Zhao Changling(赵长灵), Qin Junqing(秦均庆), Zheng Yuanyang(郑远扬),Wen Liankui(文联奎).Research based on spot experiment of treating sewage with high efficiency oil/water separator and filter[J].Environmental Protection of Oil & Gas Fields(油气田环境保护), 1998, 8(3):8-11
[20]	Qi Junqing(戚俊清), Liu Yali(刘亚莉), Xu Peiyuan(许培援), Zhang Hualin(张华林), She Qingyan(佘庆彦).Separation characteristics and experiment of inclined plate settler[J].Chemical Engineering & Machinery(化工机械), 1999,26(4):192-195
[21]	Liu Yali(刘亚莉), Xu Peiyuan(许培援), Liang Xin(梁新), Qi Junqing(戚俊清).Study on the technology of oil-water separation in inclined plate settler[J].Journal of Zhengzhou Institute of Light Industry(郑州轻工业学院学报:自然科学版), 2002,17(2):5-7
[22]	Hou Hairui(侯海瑞), Meng Huibo(孟辉波), Wu Jianhua(吴剑华).Researching on separation capability of incline plate separator[J].Journal of Shenyang Institute of Chemical Technology(沈阳化工学院学报),2006,20(3):218-221
[23]	Lars S, Michael C, Martin H, Andreas P.Liquid-liquid phase separation in gravity settler with inclined plates[J].AIChE Journal,2004,50(4):802-811

聚碳酸酯液液分离器的流体力学模拟和中试试验

Fluid dynamics simulation and pilot test for polycarbonate liquid-liquid separator

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