CIESC Journal ›› 2023, Vol. 74 ›› Issue (3): 995-1009.DOI: 10.11949/0438-1157.20221448
• Reviews and monographs • Previous Articles Next Articles
Yin XU1(), Jie CAI1, Lu CHEN1, Yu PENG1, Fuzhen LIU1(), Hui ZHANG2()
Received:
2022-11-08
Revised:
2023-01-04
Online:
2023-04-19
Published:
2023-03-05
Contact:
Fuzhen LIU, Hui ZHANG
徐银1(), 蔡洁1, 陈露1, 彭宇1, 刘夫珍1(), 张晖2()
通讯作者:
刘夫珍,张晖
作者简介:
徐银(1988—),男,博士,副教授,yxu@hubu.edu.cn
基金资助:
CLC Number:
Yin XU, Jie CAI, Lu CHEN, Yu PENG, Fuzhen LIU, Hui ZHANG. Advances in heterogeneous visible light photocatalysis coupled with persulfate activation for water pollution control[J]. CIESC Journal, 2023, 74(3): 995-1009.
徐银, 蔡洁, 陈露, 彭宇, 刘夫珍, 张晖. 异相可见光催化耦合过硫酸盐活化技术在水污染控制中的研究进展[J]. 化工学报, 2023, 74(3): 995-1009.
表征目的 | 表征内容 | 表征仪器 | 文献 |
---|---|---|---|
光响应范围 | 紫外-可见漫反射光谱(UV-Vis DRS) | 紫外-可见漫反射光谱仪 | [ |
光生载流子分离状况 | 光致发光光谱(PL) | 荧光光谱仪 | [ |
瞬时光电流(I-t) | 电化学工作站 | [ | |
光生载流子分离状况/电荷传输能力 | 电化学阻抗谱(EIS) | 电化学工作站 | [ |
循环伏安曲线(CV) | 电化学工作站 | [ | |
光生载流子的寿命 | 时间分辨光致发光光谱(TRPL) | 荧光光谱仪 | [ |
禁带宽度 | Kubelka-Munk方程式 | 紫外-可见漫反射光谱仪 | [ |
循环伏安曲线(CV) | 电化学工作站 | [ | |
密度泛函理论(DFT) | Materials Studio、VASP软件 | [ | |
价带电势 | 价带XPS能谱 | X射线光电子能谱 | [ |
导带电势 | 莫特-肖特基(Mott-Schottky)曲线 | 电化学工作站 | [ |
Table 1 Characterizations of photocatalytic material
表征目的 | 表征内容 | 表征仪器 | 文献 |
---|---|---|---|
光响应范围 | 紫外-可见漫反射光谱(UV-Vis DRS) | 紫外-可见漫反射光谱仪 | [ |
光生载流子分离状况 | 光致发光光谱(PL) | 荧光光谱仪 | [ |
瞬时光电流(I-t) | 电化学工作站 | [ | |
光生载流子分离状况/电荷传输能力 | 电化学阻抗谱(EIS) | 电化学工作站 | [ |
循环伏安曲线(CV) | 电化学工作站 | [ | |
光生载流子的寿命 | 时间分辨光致发光光谱(TRPL) | 荧光光谱仪 | [ |
禁带宽度 | Kubelka-Munk方程式 | 紫外-可见漫反射光谱仪 | [ |
循环伏安曲线(CV) | 电化学工作站 | [ | |
密度泛函理论(DFT) | Materials Studio、VASP软件 | [ | |
价带电势 | 价带XPS能谱 | X射线光电子能谱 | [ |
导带电势 | 莫特-肖特基(Mott-Schottky)曲线 | 电化学工作站 | [ |
VLP-PS体系 | 主要活性物质 | 次要活性物质 | 反应条件 | 污染物去除效率 | 文献 |
---|---|---|---|---|---|
ZnFe2O4/g-C3N4/PMS/Vis | 1O2, h+ | 0.3 g·L-1 catalyst, 0.1 mmol·L-1 双酚A, 0.5 mmol·L-1 PMS, pH 3.5~9.0 | >99.7% in 60 min | [ | |
g-C3N4/PDS/Vis | — | 0.5 g·L-1 catalyst, 5.0 mg·L-1双酚A, 5.0 mmol·L-1 PDS, pH 3 | 100% in 90 min | [ | |
g-C3N4/PMS/Vis | 0.4 g·L-1 catalyst, 20 mg·L-1 酸性橙Ⅱ, 0.2 g·L-1 PMS, pH 3.82 | 96.3% in 30 min | [ | ||
Co3O4/量子点g-C3N4/ PMS/Vis | h+, | — | 0.2 g·L-1 catalyst, 20 mg·L-1 四环素, 50 mg·L-1 PMS, pH 6 | 97.1% in 10 min | [ |
CoAl-LDHs/g-C3N4/ PMS/Vis | h+ | 0.2 g·L-1 catalyst, 10 μmol·L-1磺胺嘧啶, 0.5 mmol·L-1 PMS, pH 6.0 | 87.1% in 15 min | [ | |
Bi2O3/CuNiFe LDHs/ PDS/Vis | 0.4 g·L-1 catalyst, 10 mg·L-1 洛美沙星, 0.74 mmol·L-1 PDS, pH 6.08 | 84.6% in 40 min | [ | ||
MoO3/g-C3N4/PDS/Vis | 0.6 g·L-1 catalyst, 10 mg·L-1 氧氟沙星, 5 mmol·L-1 PDS, natural pH | 94.4% in 120 min | [ | ||
MIL-53(Fe)/PDS/Vis | — | 0.2 g·L-1 catalyst, 300 mg·L-1 四环素, 8.0 mmol·L-1 PDS, pH 3.45 | 99.7% in 80 min | [ | |
K-Fe/PDS/Vis | — | 0.4 g·L-1 catalyst, 0.1 mmol·L-1 罗丹明B, 7.0 mmol·L-1 PDS, pH 5.0 | 97.0% in 180 min | [ | |
TiO2/AB/PDS/Vis | •OH | 0.5 g·L-1 catalyst, 30 mg·L-1 四环素, 3.0 mmol·L-1 PDS, pH 4.1 | 93.3% in 120 min | [ | |
g-C3N4/Fe(Ⅲ)/PDS/Vis | — | 1.875 g·L-1 g-C3N4 with 0.35 g·L-1 Fe3+, 10 mg·L-1 苯酚, 0.3 g·L-1 PDS, natural pH | 33% in 90 min | [ | |
Co3O4/CeO2/PMS/Vis | — | 0.5 g·L-1 catalyst, 5.0 mg·L-1环丙沙星, 0.1 g·L-1 PMS, pH 3.45 | 87.8% in 50 min | [ | |
Ag/AgCl@ZIF-8/g-C3N4/PMS/Vis | 0.01 g·L-1 catalyst, 0.01 g·L-1 洛美沙星, 2.0 mmol·L-1 PMS, pH 6.5 | 87.3% in 60 min | [ | ||
Bi12O17Cl2/MIL-100(Fe)/PDS/Vis | h+, | 0.25 g·L-1 catalyst, 10 mg·L-1 双酚A, 2.0 mmol·L-1 PDS, pH 5.2 | 99.3% in 60 min | [ | |
Ilmenite/PDS/Vis | 1O2 | 1.0 g·L-1 catalyst, 5 log10 cfu·ml-1E.coli, 0.5 mmol·L-1 PDS, pH 5 | 100% in 20min | [ | |
p(HEA-APTM)-BiOI/ PMS/Vis | h+, 1O2 | 2.0 g·L-1 catalyst, 50 mg·L-1 对羟基苯甲酸甲酯, 1.5 mmol·L-1 PMS, pH 3.18 | 100% in 90min | [ | |
γ-Fe2O3/MnO2/PMS/Vis | 0.15 g·L-1 catalyst, 50 μmol·L-1 环丙沙星, 0.3 g·L-1 PMS, neutral pH | 98.3% in 30 min | [ | ||
Bi2MoO6/PDS/Vis | h+, | •OH | 0.5 g·L-1 catalyst, 20 mg·L-1 四环素, 4.0 g·L-1 PDS, pH 4.4 | 83.0% in 60 min | [ |
CuBi2O4/PMS/Vis | h+, 1O2 | 0.5 g·L-1 catalyst, 5.0 mg·L-1环丙沙星, 0.125 g·L-1 PMS, pH 5.0 | > 90% in 30 min | [ | |
g-C3N4/MnFe2O4/graphene/PDS/Vis | h+, •OH, | — | 1.0 g·L-1 catalyst, 20 mg·L-1 甲硝唑, 0.01 mol·L-1 PDS, natural pH | 94.5% in 60 min | [ |
CuBi2O4/MnO2/PMS/Vis | h+, | 0.3 g·L-1 catalyst, 10.0 mg·L-1 头孢噻呋, 0.4 g·L-1 PMS, pH 11.0 | 93.6% in 40 min | [ |
Table 2 The reactive species in VLP-PS systems
VLP-PS体系 | 主要活性物质 | 次要活性物质 | 反应条件 | 污染物去除效率 | 文献 |
---|---|---|---|---|---|
ZnFe2O4/g-C3N4/PMS/Vis | 1O2, h+ | 0.3 g·L-1 catalyst, 0.1 mmol·L-1 双酚A, 0.5 mmol·L-1 PMS, pH 3.5~9.0 | >99.7% in 60 min | [ | |
g-C3N4/PDS/Vis | — | 0.5 g·L-1 catalyst, 5.0 mg·L-1双酚A, 5.0 mmol·L-1 PDS, pH 3 | 100% in 90 min | [ | |
g-C3N4/PMS/Vis | 0.4 g·L-1 catalyst, 20 mg·L-1 酸性橙Ⅱ, 0.2 g·L-1 PMS, pH 3.82 | 96.3% in 30 min | [ | ||
Co3O4/量子点g-C3N4/ PMS/Vis | h+, | — | 0.2 g·L-1 catalyst, 20 mg·L-1 四环素, 50 mg·L-1 PMS, pH 6 | 97.1% in 10 min | [ |
CoAl-LDHs/g-C3N4/ PMS/Vis | h+ | 0.2 g·L-1 catalyst, 10 μmol·L-1磺胺嘧啶, 0.5 mmol·L-1 PMS, pH 6.0 | 87.1% in 15 min | [ | |
Bi2O3/CuNiFe LDHs/ PDS/Vis | 0.4 g·L-1 catalyst, 10 mg·L-1 洛美沙星, 0.74 mmol·L-1 PDS, pH 6.08 | 84.6% in 40 min | [ | ||
MoO3/g-C3N4/PDS/Vis | 0.6 g·L-1 catalyst, 10 mg·L-1 氧氟沙星, 5 mmol·L-1 PDS, natural pH | 94.4% in 120 min | [ | ||
MIL-53(Fe)/PDS/Vis | — | 0.2 g·L-1 catalyst, 300 mg·L-1 四环素, 8.0 mmol·L-1 PDS, pH 3.45 | 99.7% in 80 min | [ | |
K-Fe/PDS/Vis | — | 0.4 g·L-1 catalyst, 0.1 mmol·L-1 罗丹明B, 7.0 mmol·L-1 PDS, pH 5.0 | 97.0% in 180 min | [ | |
TiO2/AB/PDS/Vis | •OH | 0.5 g·L-1 catalyst, 30 mg·L-1 四环素, 3.0 mmol·L-1 PDS, pH 4.1 | 93.3% in 120 min | [ | |
g-C3N4/Fe(Ⅲ)/PDS/Vis | — | 1.875 g·L-1 g-C3N4 with 0.35 g·L-1 Fe3+, 10 mg·L-1 苯酚, 0.3 g·L-1 PDS, natural pH | 33% in 90 min | [ | |
Co3O4/CeO2/PMS/Vis | — | 0.5 g·L-1 catalyst, 5.0 mg·L-1环丙沙星, 0.1 g·L-1 PMS, pH 3.45 | 87.8% in 50 min | [ | |
Ag/AgCl@ZIF-8/g-C3N4/PMS/Vis | 0.01 g·L-1 catalyst, 0.01 g·L-1 洛美沙星, 2.0 mmol·L-1 PMS, pH 6.5 | 87.3% in 60 min | [ | ||
Bi12O17Cl2/MIL-100(Fe)/PDS/Vis | h+, | 0.25 g·L-1 catalyst, 10 mg·L-1 双酚A, 2.0 mmol·L-1 PDS, pH 5.2 | 99.3% in 60 min | [ | |
Ilmenite/PDS/Vis | 1O2 | 1.0 g·L-1 catalyst, 5 log10 cfu·ml-1E.coli, 0.5 mmol·L-1 PDS, pH 5 | 100% in 20min | [ | |
p(HEA-APTM)-BiOI/ PMS/Vis | h+, 1O2 | 2.0 g·L-1 catalyst, 50 mg·L-1 对羟基苯甲酸甲酯, 1.5 mmol·L-1 PMS, pH 3.18 | 100% in 90min | [ | |
γ-Fe2O3/MnO2/PMS/Vis | 0.15 g·L-1 catalyst, 50 μmol·L-1 环丙沙星, 0.3 g·L-1 PMS, neutral pH | 98.3% in 30 min | [ | ||
Bi2MoO6/PDS/Vis | h+, | •OH | 0.5 g·L-1 catalyst, 20 mg·L-1 四环素, 4.0 g·L-1 PDS, pH 4.4 | 83.0% in 60 min | [ |
CuBi2O4/PMS/Vis | h+, 1O2 | 0.5 g·L-1 catalyst, 5.0 mg·L-1环丙沙星, 0.125 g·L-1 PMS, pH 5.0 | > 90% in 30 min | [ | |
g-C3N4/MnFe2O4/graphene/PDS/Vis | h+, •OH, | — | 1.0 g·L-1 catalyst, 20 mg·L-1 甲硝唑, 0.01 mol·L-1 PDS, natural pH | 94.5% in 60 min | [ |
CuBi2O4/MnO2/PMS/Vis | h+, | 0.3 g·L-1 catalyst, 10.0 mg·L-1 头孢噻呋, 0.4 g·L-1 PMS, pH 11.0 | 93.6% in 40 min | [ |
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